Macroscale and Microscale Organic Experiments 7th edition by Kenneth Williamson, Katherine Masters ISBN 8214357546 9798214357546

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ISBN 10: 8214357546
ISBN 13: 9798214357546
Author: Kenneth Williamson, Katherine Masters

Succeed in your organic laboratory course with MACROSCALE AND MICROSCALE ORGANIC EXPERIMENTS, Seventh Edition. This proven, authoritative manual emphasizes safety and features new themed Modules experiments with real world applications. Using the manual’s mix of macroscale and microscale experiments, you’ll gain the knowledge and confidence you need to perform a wide variety of experiments, as well as experience working with conventionally-sized glassware.

Macroscale and Microscale Organic Experiments 7th Table of contents:

Chapter 1. Introduction

• Experimental Organic Chemistry

• Equipment for Experimental Organic Chemistry

  • Check-In of Lab Equipment

  • Transfer of Liquids and Solids

  • Weighing and Measuring

  • Tares

  • Washing and Drying Laboratory Equipment

  • Miscellaneous Cleanup

• The Laboratory Notebook

Chapter 2. Laboratory Safety, Courtesy, and Waste Disposal

• Important General Rules

• Laboratory Courtesy

• Working with Flammable Substances

• Working with Hazardous Chemicals

• Working with Explosive Hazards

• Working with Corrosive Substances

• Working with Toxic Substances

• Gloves

• Using the Laboratory Hood

• Working at Reduced Pressure

• Working with Compressed Gas Cylinders

• Odoriferous Chemicals

• Waste Disposal—Cleaning Up

• Biohazards

• Questions

Chapter 3. Melting Points and Boiling Points

Part 1: Five Concepts for Predicting Physical Properties

1. London Attractive Forces

2. Dipole–Dipole Attractive Forces

3. Hydrogen Bonding

4. Ionic Attractive Forces

5. Competing Intermolecular Forces and Solubility

Part 2: Melting Points

• Thermometers

• Melting Points

• Experimental Procedures

Part 3: Boiling Points

• Structure and Boiling Point

• Boiling Point as a Function of Pressure

• Calibrating the Thermometer

• Distillation Considerations

• Boiling Point Determination: Apparatus and Technique

• Questions

• References

Chapter 4. Recrystallization

• The Seven Steps of Recrystallization

  1. Choosing the Solvent and Solvent Pairs

  2. Dissolving the Solute

  3. Decolorizing with Norit

  4. Filtering Suspended Solids

  5. Recrystallizing the Solute

  6. Collecting and Washing the Crystals

  7. Drying the Product

Experiments

1. Solubility Tests

2. Recrystallization of Phthalic Acid, Naphthalene, and Anthracene

3. Decolorizing a Solution

4. Brown Sugar Decolorization

5. Benzoic Acid from Solvent Pair

6. Naphthalene from Mixed Solvent

7. Purification of an Unknown

• Recrystallization Problems and Solutions

• Induction of Crystallization

• Oiling Out

• Summary

• Questions

Chapter 5. Distillation

• Simple Distillation

• Fractional Distillation

• Liquid Mixtures

• Azeotropes

• Boiling Points

Experiments

1. Simple Distillation

2. Fractional Distillation

3. Instant Microscale Distillation

4. Apparatus Setup

5. Fractional Distillation of Unknowns

• Questions

• Reference

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Tags: Kenneth Williamson, Katherine Masters, Organic Experiments