How to Optimize Fluid Bed Processing Technology Part of the Expertise in Pharmaceutical Process Technology Series 1st edition by Dilip Parikh ISBN 0128047275 978-0128047279
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ISBN 10: 0128047275
ISBN 13: 978-0128047279
Author: Dilip Parikh
How to Optimize Fluid Bed Processing Technology: Part of the Expertise in Pharmaceutical Process Technology Series addresses the important components of fluid bed granulation, providing answers to problems that commonly arise and using numerous practical examples and case studies as reference.
This book covers the theoretical concepts involved in fluidization, also providing a description of the choice and functionality of equipment. Additional chapters feature key aspects of the technology, including formulation requirements, process variables, process scale-up, troubleshooting, new development, safety, and process evaluation.
Given its discussion of theoretical principles and practical solutions, this is a go-to resource for all those scientists and new researchers working with fluid bed granulation as a unit operation.
How to Optimize Fluid Bed Processing Technology Part of the Expertise in Pharmaceutical Process Technology Series 1st Table of contents:
Chapter 1. Introduction
Abstract
1.1 Introduction
1.2 Advantages and Challenges of Fluidized Bed Granulation
Chapter 2. Fluidization Theory
Abstract
2.1 How Does Fluidization Take Place?
2.2 Understanding the Particles
2.3 Types of Fluid Beds
2.4 Controlling Gas Velocity
2.5 Addressing Fluidization Challenges
2.6 Summary
References
Chapter 3. Fluid Bed Processor Equipment and Its Functionality
Abstract
3.1 Introduction
3.2 Questions Before Specifying the Equipment
3.3 Fluid Bed Processor Components
3.4 Summary
Chapter 4. Process Development
Abstract
4.1 Process Selection
4.2 Quality by Design
4.3 Processing in Fluid Bed
4.4 Risk Assessment and Management
4.5 Process Control
4.6 Case Study
4.7 Summary
Reference
Chapter 5. Granulation
Abstract
5.1 Theory
5.2 Binders
5.3 Nozzles
5.4 Process Parameters
5.5 Challenges in Fluid Bed Granulation
5.6 Granulation End Point
5.7 Granulation Characterization
5.8 Summary
References
Chapter 6. Drying
Abstract
6.1 Theory
6.2 Drying Granulated Product
6.3 Summary
References
Chapter 7. Coating
Abstract
7.1 Introduction
7.2 Top-Spray Coating
7.3 Wurster Coating
7.4 Other Coating Modules
7.5 Dry Powder Coating
7.6 Problems in Coating in Fluid Bed
7.8 Characterization of the Coating
7.9 Selection of the Process for Coating
7.10 Summary
References
Chapter 8. Pelletization
Abstract
8.1 Introduction
8.2 Pelletization With Wurster Coating Module
8.3 Pelletization in Rotary Fluid Bed
8.4 Case Studies
8.5 Characterization of Pellets
8.6 Summary
References
Chapter 9. Other Fluid Bed Processes and Applications
Abstract
9.1 Introduction
9.2 Fluidized Hot Melt Granulation (FHMG)
9.3 Spray Congealing
9.4 Pressure Swing Granulation (PSG)
9.5 Wurster Module for Granulation
9.6 Foam Granulation
9.7 Steam Granulation
9.8 Rotary Fluid Bed Agglomeration
9.9 Spray-Drying Granulation
9.10 Continuous Granulation
References
Chapter 10. Process Control and PAT
Abstract
10.1 Background
10.2 Process Control
10.3 Temperature Measurement
10.4 NIR
10.5 Chord Length Determination (FBRM and SFV)
10.6 The Lighthouse Probe
10.7 Image analysis
10.8 Other methods
10.9 Summary
References
Chapter 11. Process Scale-Up
Abstract
11.1 Introduction
11.2 Various Scale-Up Considerations and Approaches
11.3 Scale-Up of Fluid Bed Granulation and Drying
11.4 Case Studies—Granulation Scale-Up
11.5 Fluid Bed Coating Scale-Up
11.6 Rotary Fluid Bed Coating
11.7 Summary
References
Chapter 12. Integrated Systems
Abstract
12.1 Material Handling
12.2 Integrated Systems for Nonpotent Compounds
12.3 Integrated Systems for Potent Compounds
12.4 Summary
Reference
Chapter 13. Process Troubleshooting
Abstract
13.1 Troubleshooting the Granulation Process
13.2 Troubleshooting the Drying Process
13.3 Troubleshooting the Coating Process
13.4 Summary
References
Chapter 14. Fluid Bed Safety
Abstract
14.1 Introduction
14.2 Safety From Solvents
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Tags: Dilip Parikh, Optimize Fluid, the Expertise, Pharmaceutical Process