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ISBN-10 : 1305177827
ISBN-13 : 9781305177826
Author: Donald Pavia
Introduce your students to the latest advances in spectroscopy with the text that has set the standard in the field for more than three decades: INTRODUCTION TO SPECTROSCOPY, 5e, by Donald L. Pavia, Gary M. Lampman, George A. Kriz, and James R. Vyvyan. Whether you use the book as a primary text in an upper-level spectroscopy course or as a companion book with an organic chemistry text, your students will receive an unmatched, systematic introduction to spectra and basic theoretical concepts in spectroscopic methods. This acclaimed resource features up-to-date spectra; a modern presentation of one-dimensional nuclear magnetic resonance (NMR) spectroscopy; an introduction to biological molecules in mass spectrometry; and coverage of modern techniques alongside DEPT, COSY, and HECTOR.
Introduction to Spectroscopy 5th Table of contents:
Ch 1: Molecular Formulas and What Can Be Learned from Them
Introduction
1.1: Elemental Analysis and Calculations
1.2: Determination of Molecular Mass
1.3: Molecular Formulas
1.4: Index of Hydrogen Deficiency
1.5: The Rule of Thirteen
1.6: The Nitrogen Rule
Problems
References
Ch 2: Infrared Spectroscopy
Introduction
2.1: The Infrared Absorption Process
2.2: Uses of the Infrared Spectrum
2.3: The Modes of Stretching and Bending
2.4: Bond Properties and Absorption Trends
2.5: The Infrared Spectrometer
2.6: Preparation of Samples for Infrared Spectroscopy
2.7: What to Look for When Examining Infrared Spectra
2.8: Correlation Charts and Tables
2.9: How to Approach the Analysis of a Spectrum (Or What You Can Tell At a Glance)
2.10: Hydrocarbons: Alkanes, Alkenes, and Alkynes
2.11: Aromatic Rings
2.12: Alcohols and Phenols
2.13: Ethers
2.14: Carbonyl Compounds
2.15: Amines
2.16: Nitriles, Isocyanates, Isothiocyanates, and Imines
2.17: Nitro Compounds
2.18: Carboxylate Salts, Amine Salts, and Amino Acids
2.19: Sulfur Compounds
2.20: Phosphorus Compounds
2.21: Alkyl and Aryl Halides
2.22: The Background Spectrum
2.23: How to Solve Infrared Spectral Problems
Problems
References
Ch 3: Mass Spectrometry: Part One: Basic Theory, Instrumentation and Sampling Techniques
Introduction
3.1: The Mass Spectrometer: Overview
3.2: Sample Introduction
3.3: Ionization Methods
3.4: Mass Analysis
3.5: Detection and Quantitation: The Mass Spectrum
3.6: Determination of Molecular Weight
3.7: Determination of Molecular Formulas
Problems
References
Ch 4: Mass Spectrometry: Part Two: Fragmentation and Structural Analysis
Introduction
4.1: The Initial Ionization Event
4.2: Fundamental Fragmentation Processes
4.3: Fragmentation Pattern of Hydrocarbons
4.4: Fragmentation Patterns of Alcohols, Phenols, and Thiols
4.5: Fragmentation Patterns of Ethers and Sulfides
4.6: Fragmentation Patterns of Carbonyl-Containing Compounds
4.7: Fragmentation Patterns of Amines
4.8: Fragmentation Patterns of Other Nitrogen Compounds
4.9: Fragmentation Patterns of Alkyl Chlorides and Alkyl Bromides
4.10: Computerized Matching of Spectra with Spectral Libraries
4.11: Strategic Approach to Analyzing Mass Spectra and Solving Problems
4.12: How to Solve Mass Spectral Problems
References
Ch 5: Nuclear Magnetic Resonance Spectroscopy: Part One: Basic Concepts
Introduction
5.1: Nuclear Spin States
5.2: Nuclear Magnetic Moments
5.3: Absorption of Energy
5.4: The Mechanism of Absorption (Resonance)
5.5: Population Densities of Nuclear Spin States
5.6: The Chemical Shift and Shielding
5.7: The Nuclear Magnetic Resonance Spectrometer
5.8: Chemical Equivalence—A Brief Overview
5.9: Integrals and Integration
5.10: Chemical Environment and Chemical Shift
5.11: Local Diamagnetic Shielding
5.12: Magnetic Anisotropy
5.13: Spin–Spin Splitting (n + 1) Rule
5.14: The Origin of Spin–Spin Splitting
5.15: The Ethyl Group (CH3CH2–)
5.16: Pascal’s Triangle
5.17: The Coupling Constant
5.18: A Comparison of NMR Spectra at Low- and High-Field Strengths
5.19: Survey of Typical 1H NMR Absorptions by Type of Compound
5.20: How to Solve NMR Spectra Problems
Problems
References
Ch 6: Nuclear Magnetic Resonance Spectroscopy: Part Two: Carbon-13 Spectra, Including Heteronuclear
Introduction
6.1: The Carbon-13 Nucleus
6.2: Carbon-13 Chemical Shifts
6.3: Proton-Coupled 13C Spectra—Spin–Spin Splitting of Carbon-13 Signals
6.4: Proton-Decoupled 13C Spectra
6.5: Nuclear Overhauser Enhancement (NOE)
6.6: Cross-Polarization: Origin of the Nuclear Overhauser Effect
6.7: Problems with Integration in 13C Spectra
6.8: Molecular Relaxation Processes
6.9: Off-Resonance Decoupling
6.10: A Quick Dip into DEPT
6.11: Some Sample Spectra—Equivalent Carbons
6.12: Nonequivalent Carbon Atoms
6.13: Compounds with Aromatic Rings
6.14: Carbon-13 NMR Solvents—Heteronuclear Coupling of Carbon to Deuterium
6.15: Heteronuclear Coupling of Carbon-13 to Fluorine-19
6.16: Heteronuclear Coupling of Carbon-13 to Phosphorus-31
6.17: Carbon and Proton NMR: How to Solve a Structure Problem
Problems
References
Ch 7: Nuclear Magnetic Resonance Spectroscopy: Part Three: Spin–Spin Coupling
Introduction
7.1: Coupling Constants: Symbols
7.2: Coupling Constants: The Mechanism of Coupling
7.3: Magnetic Equivalence
7.4: Spectra of Diastereotopic Systems
7.5: Nonequivalence within a Group—The Use of Tree Diagrams when the n + 1 Rule Fails
7.6: Measuring Coupling Constants from First-Order Spectra
7.7: Second-Order Spectra—Strong Coupling
7.8: Alkenes
7.9: Measuring Coupling Constants—Analysis of an Allylic System
7.10: Aromatic Compounds—Substituted Benzene Rings
7.11: Coupling in Heteroaromatic Systems
7.12: Heteronuclear Coupling of 1H TO 19F and 31P
7.13: How to Solve Problems Involving Coupling Constant Analysis
Problems
References
Ch 8: Nuclear Magnetic Resonance Spectroscopy: Part Four: Other Topics in One-Dimensional NMR
Introduction
8.1: Protons on Oxygen: Alcohols
8.2: Exchange in Water and D2O
8.3: Other Types of Exchange: Tautomerism
8.4: Protons on Nitrogen: Amines
8.5: Protons on Nitrogen: Quadrupole Broadening and Decoupling
8.6: Amides
8.7: Solvent Effects
8.8: Chemical Shift Reagents
8.9: Chiral Resolving Agents
8.10: Determining Absolute and Relative Configuration via NMR
8.11: Nuclear Overhauser Effect Difference Spectra
8.12: How to Solve Problems Involving Advanced 1-D Methods
Problems
References
Ch 9: Nuclear Magnetic Resonance Spectroscopy: Part Five: Advanced NMR Techniques
Introduction
9.1: Pulse Sequences
9.2: Pulse Widths, Spins, and Magnetization Vectors
9.3: Pulsed Field Gradients
9.4: The DEPT Experiment: Number of Protons Attached to 13C Atoms
9.5: Determining the Number of Attached Hydrogens
9.6: Introduction to Two-Dimensional Spectroscopic Methods
9.7: The COSY Technique: 1H-1H Correlations
9.8: The HETCOR Technique: 1H-13C Correlations
9.9: Inverse Detection Methods
9.10: The NOESY Experiment
9.11: Magnetic Resonance Imaging
9.12: Solving a Structural Problem Using Combined 1-D and 2-D Techniques
Problems
References
Ch 10: Ultraviolet Spectroscopy
Introduction
10.1: The Nature of Electronic Excitations
10.2: The Origin of UV Band Structure
10.3: Principles of Absorption Spectroscopy
10.4: Instrumentation
10.5: Presentation of Spectra
10.6: Solvents
10.7: What Is a Chromophore?
10.8: The Effect of Conjugation
10.9: The Effect of Conjugation on Alkenes
10.10: The Woodward–Fieser Rules for Dienes
10.11: Carbonyl Compounds; Enones
10.12: Woodward’s Rules for Enones
10.13: α,β-Unsaturated Aldehydes, Acids, and Esters
10.14: Aromatic Compounds
10.15: Model Compound Studies
10.16: Visible Spectra: Color in Compounds
10.17: What to Look for in an Ultraviolet Spectrum: A Practical Guide
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