Ion Exchange and Solvent Extractionv 1st edition by Bruce Moyer – Ebook PDF Instant Download/Delivery: 1040213131 , 9781040213131
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ISBN 10: 1040213131
ISBN 13: 9781040213131
Author: Bruce Moyer
Over the past several decades, the theme of supramolecular chemistry (SC) has permeated nearly all aspects of chemical endeavor. Not surprisingly, it has also pervaded the field of solvent extraction (SX), inspiring the framework for this volume of Ion Exchange and Solvent Extraction. In addition, tools for studying aggregation have grown increasin
Ion Exchange and Solvent Extractionv 1st Table of contents:
Chapter 1 Supramolecular Chemistry in Solvent Extraction: Toward Highly Selective Extractants and a Better Understanding of Phase-Transfer Phenomena
1.1 Introduction
1.2 Supramolecular Chemistry in Relation to Solvent Extraction
1.2.1 What is Supramolecular Chemistry?
1.2.2 Supramolecular Aspects of Solvent Extraction Systems
1.3 Selected Examples Illustrating Supramolecular Concepts in Action
1.3.1 Cation Binding and Extraction
1.3.1.1 Solvent Extraction Employing Mixed Extractants
1.3.1.2 Dendritic Cation Extractants
1.3.2 Anion Binding and Extraction
1.3.2.1 General Considerations
1.3.2.2 Uncharged Anion Receptors
1.3.2.3 Charged Anion Receptors
1.3.2.4 Dendritic Anion Extractants
1.3.3 Ion-Pair Receptors
1.3.4 Small-Molecule Binding and Extraction
1.4 Further Considerations
Acknowledgments
References
Chapter 2 Supramolecular Interactions in the Outer Coordination Spheres of Extracted Metal Ions
2.1 Introduction
2.2 Extraction of Metal Cations
2.3 Extraction of Metalate Anions
2.4 Metal Salt Extraction
2.5 Conclusions
Acknowledgments
References
Chapter 3 Molecular Design and Metal Extraction Behavior of Calixarene Compounds as Host Extractants
3.1 Introduction
3.2 Macrocyclic Ligands
3.2.1 Structures and Names of the Compounds
3.2.2 Characteristics of Calixarenes
3.3 Molecular Design of Calixarene Compounds For Metal Extraction
3.4 Research On Metal Cation Extraction With Calixarene Derivatives
3.5 Conclusions
References
Chapter 4 Protein Extraction by the Recognition of Lysine Residues Using Macrocyclic Molecules
4.1 Introduction
4.2 Protein Extraction Using Calixarenes
4.2.1 Recognition of Biomolecules Using Calixarenes
4.2.2 Protein Extraction Using Calixarenes
4.2.3 Separation of Proteins Using Calixarene
4.2.4 Protein Refolding via Liquid–Liquid Extraction Using Calixarene
4.2.5 Enzymatic Reaction of Extracted Proteins in Organic Media
4.3 Protein Extraction Using Crown Ethers
4.3.1 Dissolution of Proteins in Organic Media Using Crown Ethers
4.3.2 Extraction of Proteins in an Ionic Liquid System
4.3.3 Extraction of Proteins in an Aqueous Two-Phase System
4.4 Perspective
References
Chapter 5 Interfacial Molecular Aggregation in Solvent Extraction Systems
5.1 Introduction
5.2 Formation of Aggregates And Micelles in Solvent Extraction Systems
5.2.1 Aggregation of Amines and Ammonium Salts
5.2.2 Aggregation of Acidic Extractants
5.2.3 Aggregation of Coordinating Extractants and Others
5.3 Formation of Microemulsions And Microdroplets in Solvent Extraction Systems
5.4 Molecular Aggregation At Liquid–Liquid Interfaces
5.4.1 Studies by Conventional Methods
5.4.2 Studies by Newly Developed Experimental Methods
5.4.2.1 High-Speed Stirring (HSS) Method
5.4.2.2 Centrifugal Liquid–Membrane (CLM) Method
5.4.2.3 Total Interfacial Reflection Spectroscopy
5.4.2.4 Raman Spectroscopy of Liquid–Liquid Interface
5.4.2.5 Optical Chirality Measurement
5.4.2.6 Second Harmonic Generation Spectroscopy
5.4.2.7 Magnetophoretic Measurement of Interfacial Aggregates
5.5 Computer Simulation of Interfacial Aggregation
5.6 Summary
Acknowledgments
References
Chapter 6 Supramolecular Aspects of Stable Water-in-Oil Microemulsions in Chemical Separations
6.1 Introduction
6.2 Experimental And Analytical Considerations For Sx Systems With Extensive Aggregative Behavior
6.3 General Observations For Liquid–Liquid Extraction Systems
6.3.1 Solvent-Centered versus Metal-Centered Extraction
6.3.2 Thermodynamic Observations in Extraction Systems
6.3.3 Metal Distribution Observations in Microemulsion Systems
6.4 Behavior of Extractants in Specific Systems
6.4.1 Neutral Organophosphorous Extractants
6.4.1.1 TBP
6.4.1.2 TRPO (TOPO, etc.)
6.4.2 Amides
6.4.2.1 Monoamides
6.4.2.2 Diamides
6.4.2.3 Diglycolamides
6.4.3 Acidic Organophosphorous Extractants
6.4.3.1 HDEHP
6.4.3.2 Alkylenediphosphonic Acids
6.4.4 Surfactant Systems and Synergistic Extraction Systems
6.5 Outlook
6.6 Summary
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