Laboratory Methods in Dynamic Electroanalysis 1st edition by Teresa Fernández Abedul – Ebook PDF Instant Download/Delivery: 0128159330 , 9780128159330
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ISBN 10: 0128159330
ISBN 13: 9780128159330
Author: Teresa Fernández Abedul
Laboratory Methods in Dynamic Electroanalysis is a useful guide to introduce analytical chemists and scientists of related disciplines to the world of dynamic electroanalysis using simple and low-cost methods. The trend toward decentralization of analysis has made this fascinating field one of the fastest-growing branches of analytical chemistry. As electroanalytical devices have moved from conventional electrochemical cells (10-20 mL) to current cells (e.g. 5-50 mL) based on different materials such as paper or polymers that integrate thick- or thin-film electrodes, interesting strategies have emerged, such as the combination of microfluidic cells and biosensing or nanostructuration of electrodes.
This book provides detailed, easy procedures for dynamic electroanalysis and covers the main trends in electrochemical cells and electrodes, including microfluidic electrodes, electrochemical detection in microchip electrophoresis, nanostructuration of electrodes, development of bio (enzymatic, immuno, and DNA) assays, paper-based electrodes, interdigitated array electrodes, multiplexed analysis, and combination with optics. Different strategies and techniques (amperometric, voltammetric, and impedimetric) are presented in a didactic, practice-based way, and a bibliography provides readers with additional sources of information.
- Provides easy-to-implement experiments using low-cost, simple equipment
- Includes laboratory methodologies that utilize both conventional designs and the latest trends in dynamic electroanalysis
- Goes beyond the fundamentals covered in other books, focusing instead on practical applications of electroanalysis
Laboratory Methods in Dynamic Electroanalysis 1st Table of contents:
Chapter 1. Dynamic electroanalysis: an overview
1.1. Dynamic electroanalysis
1.2. Additional notes
I. Dynamic electroanalytical techniques
Chapter 2. Determination of ascorbic acid in dietary supplements by cyclic voltammetry
2.1. Background
2.2. Electrochemical cell
2.3. Chemicals and supplies
2.4. Hazards
2.5. Experimental procedure
2.6. Lab report
2.7. Additional notes
2.8. Assessment and discussion questions
Chapter 3. Electrochemical behavior of the redox probe hexaammineruthenium(III) ([Ru(NH3)6]3+) using voltammetric techniques
3.1. Background
3.2. Electrochemical cell
3.3. Chemicals and supplies
3.4. Hazards
3.5. Experimental procedure
3.6. Lab report
3.7. Additional notes
3.8. Assessment and discussion questions
Chapter 4. Anodic stripping voltammetric determination of lead and cadmium with stencil-printed transparency electrodes
4.1. Background
4.2. Electrochemical cell design
4.3. Chemicals and supplies
4.4. Hazards
4.5. Experimental procedure
4.6. Lab report
4.7. Additional notes
4.8. Assessment and discussion questions
Chapter 5. Adsorptive stripping voltammetry of indigo blue in a flow system
5.1. Background
5.2. Chemicals and supplies
5.3. Hazards
5.4. Flow injection analysis electrochemical system
5.5. Experimental procedures
5.6. Lab report
5.7. Additional notes
5.8. Assessment and discussion questions
Chapter 6. Enhancing electrochemical performance by using redox cycling with interdigitated electrodes
6.1. Background
6.2. Chemicals and supplies
6.3. Hazards
6.4. Electrochemical system setup
6.5. Experimental procedure
6.6. Lab report
6.7. Additional notes
6.8. Assessment and discussion questions
Chapter 7. Amperometric detection of NADH using carbon-based electrodes
7.1. Background
7.2. Chemicals and supplies
7.3. Hazards
7.4. Experimental procedure
7.5. Lab report
7.6. Additional notes
7.7. Assessment and discussion questions
Chapter 8. Chronoamperometric determination of ascorbic acid on paper-based devices
8.1. Background
8.2. Electrochemical cell design
8.3. Chemicals and supplies
8.4. Hazards
8.5. Experimental procedure
8.6. Lab report
8.7. Additional notes
8.8. Assessment and discussion questions
Chapter 9. Electrochemical detection of melatonin in a flow injection analysis system
9.1. Background
9.2. Electrochemical thin-layer cell
9.3. Flow injection analysis system
9.4. Chemicals and supplies
9.5. Hazards
9.6. Experimental procedure
9.7. Lab report
9.8. Additional notes
9.9. Assessment and discussion questions
Chapter 10. Batch injection analysis for amperometric determination of ascorbic acid at ruthenium dioxide screen-printed electrodes
10.1. Background
10.2. Chemicals and supplies
10.3. Hazards
10.4. Experimental procedure
10.5. Lab report
10.6. Additional notes
10.7. Assessment and discussion questions
Chapter 11. Impedimetric aptasensor for determination of the antibiotic neomycin B
11.1. Background
11.2. Chemicals and supplies
11.3. Hazards
11.4. Experimental procedure
11.5. Lab report
11.6. Additional notes
11.7. Assessment and discussion questions
Chapter 12. Electrochemical impedance spectroscopy for characterization of electrode surfaces: carbon nanotubes on gold electrodes
12.1. Background
12.2. Electrochemical cell
12.3. Chemicals and supplies
12.4. Hazards
12.5. Electrochemical procedure
12.6. Lab report
12.7. Additional notes
12.8. Assessment and discussion questions
II. Electroanalysis and microfluidics
Chapter 13. Single- and dual-channel hybrid PDMS/glass microchip electrophoresis device with amperometric detection
13.1. Background
13.2. Chemicals and supplies
13.3. Microchip fabrication
13.4. Microchip designs
13.5. Electrochemical detector design
13.6. Hazards
13.7. Experimental procedure
13.8. Lab report
13.9. Additional notes
13.10. Assessment and discussion questions
Chapter 14. Analysis of uric acid and related compounds in urine samples by electrophoresis in microfluidic chips
14.1. Background
14.2. Electrophoresis system setup
14.3. Chemicals and supplies
14.4. Hazards
14.5. Experimental procedure
14.6. Lab report
14.7. Additional notes
14.8. Assessment and discussion questions
Chapter 15. Microchannel modifications in microchip reverse electrophoresis for ferrocene carboxylic acid determination
15.1. Background
15.2. Electrophoresis microchip
15.3. Chemicals and supplies
15.4. Hazards
15.5. Experimental procedure
15.6. Lab report
15.7. Additional notes
15.8. Assessment and discussion questions
Chapter 16. Integrated microfluidic electrochemical sensors to enhance automated flow analysis systems
16.1. Background
16.2. Flow injection analysis system setup
16.3. Chemicals and supplies
16.4. Hazards
16.5. Experimental procedure
16.6. Lab report
16.7. Additional notes
16.8. Assessment and discussion questions
III. Bioelectroanalysis
Chapter 17. Bienzymatic amperometric glucose biosensor
17.1. Background
17.2. Electrochemical setup
17.3. Chemicals and supplies
17.4. Hazards
17.5. Experimental procedure
17.6. Lab report
17.7. Additional notes
17.8. Assessment and discussion questions
Chapter 18. Determination of ethyl alcohol in beverages using an electrochemical enzymatic sensor
18.1. Background
18.2. Electrochemical setup
18.3. Chemicals and supplies
18.4. Hazards
18.5. Experimental procedure
18.6. Lab report
18.7. Additional notes
18.8. Assessment and discussion questions
Chapter 19. Enzymatic determination of ethanol on screen-printed cobalt phthalocyanine/carbon electrodes
19.1. Background
19.2. Electrochemical cell
19.3. Chemical and supplies
19.4. Hazards
19.5. Experimental procedure
19.6. Lab report
19.7. Additional notes
19.8. Assessment and discussion questions
Chapter 20. Immunoelectroanalytical assay based on the electrocatalytic effect of gold labels on silver electrodeposition
20.1. Background
20.2. Electrochemical cells
20.3. Chemicals and supplies
20.4. Hazards
20.5. Experimental procedures
20.6. Lab report
20.7. Additional notes
20.8. Assessment and discussion questions
Chapter 21. Genosensor on gold films with enzymatic electrochemical detection of a SARS virus sequence
21.1. Background
21.2. Electrochemical cell
21.3. Chemicals and supplies
21.4. Hazards
21.5. Experimental procedures
21.6. Lab report
21.7. Additional notes
21.8. Assessment and discussion questions
Chapter 22. Aptamer-based magnetoassay for gluten determination
22.1. Background
22.2. Chemical and supplies
22.3. Hazards
22.4. Experimental procedure
22.5. Lab report
22.6. Additional notes
22.7. Assessment and discussion questions
IV. Nanomaterials and electroanalysis
Chapter 23. Determination of lead with electrodes nanostructured with gold nanoparticles
23.1. Background
23.2. Electrochemical cell
23.3. Chemicals and supplies
23.4. Hazards
23.5. Experimental procedure
23.6. Lab report
23.7. Additional notes
23.8. Assessment and discussion questions
Chapter 24. Electrochemical behavior of the dye methylene blue on screen-printed gold electrodes modified with carbon nanotubes
24.1. Background
24.2. Screen-printed gold electrodes
24.3. Chemicals and supplies
24.4. Hazards
24.5. Experimental procedure
24.6. Lab report
24.7. Additional notes
24.8. Assessment and discussion questions
V. Low-cost electroanalysis
Chapter 25. Determination of glucose with an enzymatic paper-based sensor
25.1. Background
25.2. Electrochemical cell design
25.3. Chemical and supplies
25.4. Hazards
25.5. Experimental procedure
25.6. Lab report
25.7. Additional notes
25.8. Assessment and discussion questions
Chapter 26. Determination of arsenic (III) in wines with nanostructured paper-based electrodes
26.1. Background
26.2. Chemicals and supplies
26.3. Hazards
26.4. Experimental procedure
26.5. Lab report
26.6. Additional notes
26.7. Assessment and discussion questions
Chapter 27. Pin-based electrochemical sensor
27.1. Background
27.2. Electrochemical cell design
27.3. Chemicals and supplies
27.4. Hazards
27.5. Experimental procedure
27.6. Lab report
27.7. Additional notes
27.8. Assessment and discussion questions
Chapter 28. Flow injection electroanalysis with pins
28.1. Background
28.2. Flow injection analysis and electrochemical cell design
28.3. Chemical and supplies
28.4. Hazards
28.5. Experimental procedure
28.6. Lab report
28.7. Additional notes
28.8. Assessment and discussion questions
Chapter 29. Staple-based paper electrochemical platform for quantitative analysis
29.1. Background
29.2. Electrochemical setup
29.3. Chemicals and supplies
29.4. Hazards
29.5. Experimental procedure
29.6. Lab report
29.7. Additional notes
29.8. Assessment and discussion questions
VI. Multiplexed electroanalysis
Chapter 30. Simultaneous measurements with a multiplexed platform containing eight electrochemical cells
30.1. Background
30.2. Electrochemical platform
30.3. Chemical and supplies
30.4. Hazards
30.5. Experimental procedure
30.6. Lab report
30.7. Additional notes
30.8. Assessment and discussion questions
Chapter 31. Simultaneous detection of bacteria causing community-acquired pneumonia by genosensing
31.1. Background
31.2. Electrochemical cell design
31.3. Chemicals and supplies
31.4. Hazards
31.5. Experimental procedure
31.6. Lab report
31.7. Additional notes
31.8. Assessment and discussion questions
VII. Spectroelectrochemical techniques
Chapter 32. Electrochemiluminescence of tris (1,10-phenanthroline) ruthenium(II) complex with multipulsed amperometric detection
32.1. Background
32.2. Chemicals and supplies
32.3. Hazards
32.4. Experimental procedure
32.5. Lab report
32.6. Additional notes
32.7. Assessment and discussion questions
Chapter 33. Detection of hydrogen peroxide by flow injection analysis based on electrochemiluminescence resonance energy transfer donor–acceptor strategy
33.1. Background
33.2. Chemicals and supplies
33.3. Hazards
33.4. Experimental procedure
33.5. Lab report
33.6. Additional notes
33.7. Assessment and discussion questions
Chapter 34. Determination of tris(bipyridine)ruthenium(II) based on electrochemical surface-enhanced raman scattering
34.1. Background
34.3. Chemicals and supplies
34.4. Hazards
34.5. Experimental procedure
34.6. Lab report
34.7. Additional notes
34.8. Assessment and discussion questions
VIII. General considerations
Chapter 35. Design of experiments at electroanalysis. Application to the optimization of nanostructured electrodes for sensor development
35.1. Background
35.2. Electrochemical cell
35.3. Chemicals and supplies
35.4. Hazards
35.5. Experimental procedure
35.6. Lab report
35.7. Additional notes
35.8. Assessment and discussion questions
Chapter 36. Bibliographic resources in electroanalysis
36.1. Books and monographs
36.2. Journals
36.3. Web resources
Index
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Tags: Teresa Fernández Abedul, Laboratory Methods, Dynamic Electroanalysis